A high-pressure study of PbCO<SUB>3</SUB> by XRD and Raman spectroscopy

ZHANG Yu-Feng; LIU Jing; QIN Zhen-Xing; LIN Chuan-Long; XIONG Lun; LI Rui; BAI Li-Gang

doi:10.1088/1674-1137/37/3/038001

Chinese Physics C> 2013, Vol. 37> Issue(3) : 038001 DOI: 10.1088/1674-1137/37/3/038001

A high-pressure study of PbCO₃ by XRD and Raman spectroscopy

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Abstract：
The pressure-induced phase transitions of PbCO₃ are studied using synchrotron radiation in a diamond anvil cell at room temperature. The XRD measurement indicates that PbCO₃ with an initial phase of aragonite-type structure undergoes two phase transitions at ～ 7.8 GPa and ～ 15.7 GPa，respectively. The higher-pressure phase appearing at ～ 15.7 GPa is stable up to 51.8 GPa. The two phase transitions are further confirmed by Raman scattering up to 23.3 GPa. During the decompression process, the high-pressure phases of PbCO₃ are gradually recovered to the starting aragonite-type structure, but exhibit some hysteresis. The bulk modulus B₀ of the aragonite-type structure is obtained to be 63± (3) GPa by fitting the volume-pressure data to the Birch-Murnaghan equation of states with B₀' fixed to 4.

References

[1]

Moses W W et al. IEEE Transactions on Nuclear Science, 1991, 38: 648-653[2] BAO Y F et al. Battery Bimonthly, 2002, 32: 230-232[3] Bakhman N N et al. Combustion and Flame, 1971，17: 383-389[4] Speer J A et al. Carbonates: Mineralgoy and Chemistry. Washington D C, 1983. 145-190[5] Chevrier G et al. Zeitschrift fur Kristallographie, 1992, 199: 67-74[6] Sytle M ANTAO et al. the Canadian Mineralogist, 2009, 47: 1245-1255[7] LIN C C et al. J. Phys. Chem. Sol., 1997b, 58: 977-987[8] LIN C C et al. Phys. Chem. Miner., 1997a, 24: 149-157[9] Catalli K, Santillian J et al. Phys. Chem. Miner., 2005, 32: 412-417[10] Robert Minch et al. Phys. Chem. Miner., 2010, 37: 45-56[11] MAO H K, XU J, Bell P M et al. J. Geophys. Res., 1986, 91: 4673-4676[12] Hammersley A P et al. High Press Res., 1996, 14: 235-248[13] Larson A C, Von Dreele R B. General Structure Analysis System, Los Alamos National Laboratory Report LAUR, 2004. 86-748[14] Aderson O L. Equation of State of Solids for Geophysics and Ceramic Science. New York: Oxford University, 1995.[15] Herman R G, Bogdan C E et al. Appl. Spectrosc., 1987, 41: 437-440[16] Coleyshaw E E, Griffith W P et al. Spectrochimica Acta, 1994, 50A: 1909-1918

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ZHANG Yu-Feng, LIU Jing, QIN Zhen-Xing, LIN Chuan-Long, XIONG Lun, LI Rui and BAI Li-Gang. A high-pressure study of PbCO₃ by XRD and Raman spectroscopy[J]. Chinese Physics C, 2013, 37(3): 038001. doi: 10.1088/1674-1137/37/3/038001

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Received: 2012-04-18
Revised: 2012-06-07

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通讯作者: 陈斌, bchen63@163.com

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沈阳化工大学材料科学与工程学院沈阳 110142

A high-pressure study of PbCO₃ by XRD and Raman spectroscopy

Corresponding author: ZHANG Yu-Feng,

Corresponding author: LIU Jing,

Received Date: 2012-04-18

Accepted Date: 2012-06-07

Available Online: 2013-03-05

Abstract: The pressure-induced phase transitions of PbCO₃ are studied using synchrotron radiation in a diamond anvil cell at room temperature. The XRD measurement indicates that PbCO₃ with an initial phase of aragonite-type structure undergoes two phase transitions at ～ 7.8 GPa and ～ 15.7 GPa，respectively. The higher-pressure phase appearing at ～ 15.7 GPa is stable up to 51.8 GPa. The two phase transitions are further confirmed by Raman scattering up to 23.3 GPa. During the decompression process, the high-pressure phases of PbCO₃ are gradually recovered to the starting aragonite-type structure, but exhibit some hysteresis. The bulk modulus B₀ of the aragonite-type structure is obtained to be 63± (3) GPa by fitting the volume-pressure data to the Birch-Murnaghan equation of states with B₀' fixed to 4.

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A high-pressure study of PbCO₃ by XRD and Raman spectroscopy

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A high-pressure study of PbCO₃ by XRD and Raman spectroscopy

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A high-pressure study of PbCO3 by XRD and Raman spectroscopy

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A high-pressure study of PbCO3 by XRD and Raman spectroscopy

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A high-pressure study of PbCO₃ by XRD and Raman spectroscopy

A high-pressure study of PbCO₃ by XRD and Raman spectroscopy