A high-pressure study of PbCO<SUB>3</SUB> by XRD and Raman spectroscopy

ZHANG Yu-Feng; LIU Jing; QIN Zhen-Xing; LIN Chuan-Long; XIONG Lun; LI Rui; BAI Li-Gang

doi:10.1088/1674-1137/37/3/038001

Chinese Physics C> 2013, Vol. 37> Issue(3) : 038001 DOI: 10.1088/1674-1137/37/3/038001

A high-pressure study of PbCO₃ by XRD and Raman spectroscopy

Abstract
HTML
Reference
Related

PDF

Abstract：
The pressure-induced phase transitions of PbCO₃ are studied using synchrotron radiation in a diamond anvil cell at room temperature. The XRD measurement indicates that PbCO₃ with an initial phase of aragonite-type structure undergoes two phase transitions at ～ 7.8 GPa and ～ 15.7 GPa，respectively. The higher-pressure phase appearing at ～ 15.7 GPa is stable up to 51.8 GPa. The two phase transitions are further confirmed by Raman scattering up to 23.3 GPa. During the decompression process, the high-pressure phases of PbCO₃ are gradually recovered to the starting aragonite-type structure, but exhibit some hysteresis. The bulk modulus B₀ of the aragonite-type structure is obtained to be 63± (3) GPa by fitting the volume-pressure data to the Birch-Murnaghan equation of states with B₀' fixed to 4.

References

[1]

Moses W W et al. IEEE Transactions on Nuclear Science, 1991, 38: 648-653[2] BAO Y F et al. Battery Bimonthly, 2002, 32: 230-232[3] Bakhman N N et al. Combustion and Flame, 1971，17: 383-389[4] Speer J A et al. Carbonates: Mineralgoy and Chemistry. Washington D C, 1983. 145-190[5] Chevrier G et al. Zeitschrift fur Kristallographie, 1992, 199: 67-74[6] Sytle M ANTAO et al. the Canadian Mineralogist, 2009, 47: 1245-1255[7] LIN C C et al. J. Phys. Chem. Sol., 1997b, 58: 977-987[8] LIN C C et al. Phys. Chem. Miner., 1997a, 24: 149-157[9] Catalli K, Santillian J et al. Phys. Chem. Miner., 2005, 32: 412-417[10] Robert Minch et al. Phys. Chem. Miner., 2010, 37: 45-56[11] MAO H K, XU J, Bell P M et al. J. Geophys. Res., 1986, 91: 4673-4676[12] Hammersley A P et al. High Press Res., 1996, 14: 235-248[13] Larson A C, Von Dreele R B. General Structure Analysis System, Los Alamos National Laboratory Report LAUR, 2004. 86-748[14] Aderson O L. Equation of State of Solids for Geophysics and Ceramic Science. New York: Oxford University, 1995.[15] Herman R G, Bogdan C E et al. Appl. Spectrosc., 1987, 41: 437-440[16] Coleyshaw E E, Griffith W P et al. Spectrochimica Acta, 1994, 50A: 1909-1918

[1]	Virendrasinh Kher , Ajay Kumar Rai . Spectroscopy and decay properties of charmonium. Chinese Physics C, 2018, 42(8): 083101. doi: 10.1088/1674-1137/42/8/083101
[2]	CHEN Si , HUANG Sen-Lin , LIU Ke-Xin , CHEN Jia-Er . Beam breakup simulation study for a high energy ERL. Chinese Physics C, 2015, 39(1): 017006. doi: 10.1088/1674-1137/39/1/017006
[3]	FANG Lei-Ming , CHEN Xi-Ping , SUN Guang-Ai , CHEN Bo , PENG Shu-Ming . Formation of diamond powders from melamine under high pressure and high temperature. Chinese Physics C, 2013, 37(8): 088002. doi: 10.1088/1674-1137/37/8/088002
[4]	WANG Jing-Shu , MA Chun-Li , ZHU Hong-Yang , WU Xiao-Xin , LI Dong-Mei , CONG Ri-Dong , LIU Jing , SHI Rui , CUI Qi-Liang . Structural transition of BaF₂ nanocrystals under high pressure. Chinese Physics C, 2013, 37(8): 088001. doi: 10.1088/1674-1137/37/8/088001
[5]	ZHANG Xiao-Li , WU Ye , ZHANG Qian , DONG Jun-Cai , WU Xiang , LIU Jing , WU Zi-Yu , CHEN Dong-Liang . Pressure-induced phase transitions of multiferroic BiFeO₃. Chinese Physics C, 2013, 37(12): 128001. doi: 10.1088/1674-1137/37/12/128001
[6]	LIU Bo , LIU Ran , LI Quan-Jun , YAO Ming-Guang , ZOU Bo , CUI Tian , LIU Bing-Bing , LIU Jing . Study of high pressure structural stability of CeO₂ nanoparticles. Chinese Physics C, 2013, 37(9): 098003. doi: 10.1088/1674-1137/37/9/098003
[7]	LIU Jun-Hui , LI Dao-Wu , ZHANG Zhi-Ming , WANG Bao-Yi , ZHANG Tian-Bao , HAO Jia , WEI Long . Using a LaBr₃:Ce scintillator for positron annihilation lifetime spectroscopy. Chinese Physics C, 2012, 36(4): 380-383. doi: 10.1088/1674-1137/36/4/016
[8]	FAN Da-Wei , MA Mai-Ning , WEI Shu-Yi , CHEN Zhi-Qiang , XIE Hong-Sen . Synchrotron X-ray diffraction study of phenacite at high pressure. Chinese Physics C, 2012, 36(2): 179-183. doi: 10.1088/1674-1137/36/2/014
[9]	SONG Yu-Shou , Margaryan A , HU Bi-Tao , TANG Li-Guang . Performance of the low pressure MWPCs for fission fragments under a high background. Chinese Physics C, 2011, 35(8): 758-762. doi: 10.1088/1674-1137/35/8/011
[10]	LIU Chun-Bao , WANG Zhi-Guang . Raman scattering investigation of C-doped a-SiO₂ after high energy heavy ion irradiations. Chinese Physics C, 2011, 35(9): 885-889. doi: 10.1088/1674-1137/35/9/019
[11]	LIU Ying-Xin , QIN Shan , WU Xiang , JIANG Jian-Zhong , Kikegawa Takumi , SHI Guang-Hai . High pressure X-ray diffraction study of SrMnO₃ perovskite. Chinese Physics C, 2011, 35(5): 514-518. doi: 10.1088/1674-1137/35/5/022
[12]	LIU Ying-Xin , QIN Shan , JIANG Jian-Zhong , Kikegawa Takumi , SHI Guang-Hai . High pressure X-ray diffraction study of CaMnO₃ perovskite. Chinese Physics C, 2010, 34(7): 1025-1028. doi: 10.1088/1674-1137/34/7/018
[13]	XU Tao , HUANG Lei , DONG Yan-Guo , LI Gong , LI Yan-Chun , LIU Jing , LIU Ri-Ping . In situ X-ray diffraction investigation of compression behavior in Gd₄₀Y₁₆Al₂₄Co₂₀ bulk metallic glass under high pressure with synchrotronradiation. Chinese Physics C, 2009, 33(11): 1028-1032. doi: 10.1088/1674-1137/33/11/020
[14]	ZHENG Li-Rong , CHE Rong-Zheng , LIU Jing , DU Yong-Hua , ZHOU Ying-Li , HU Tian-Dou . A new cell for X-ray absorption spectroscopy study under high pressure. Chinese Physics C, 2009, 33(8): 701-705. doi: 10.1088/1674-1137/33/8/020
[15]	HUA Zheng-Dong , XU Xun-Jiang , WANG Jian-Hua , LIU Shu-Dong , LI Jian-Ping . Study of the energy response of high pressure ionization chamber for high energy gamma-ray. Chinese Physics C, 2008, 32(5): 370-372. doi: 10.1088/1674-1137/32/5/008
[16]	CUI Yan-Li , YI Rong-Qing , DU Hua-Bing , ZHAO Yi-Dong , CUI Ming-Qi , ZHENG Lei . Calibration of XRD Detector and Filter on the 3B3 Medium Energy X-Ray Beam in BSRF. Chinese Physics C, 2006, 30(9): 912-915.
[17]	ZHOU Qiang , HE Zhi , LI Fang-Fei , ZHANG Jian , LI Xue-Fei , MA Yan-Mei , PENG Gang , CUI Qi-Liang , LIU Jing , ZOU Guang-Tian . High-Temperature High-Pressure Synchrotron X-Ray Diffraction Study of C₃N₄. Chinese Physics C, 2005, 29(S1): 126-129.
[18]	ZHANG Wei-Wei , CUI Qi-Liang , PANG Yue-Wu , ZHU Pin-Wen , MA Hong-An , ZOU Guang-Tian , LIU Jing , LI Yan-Chun , LI Xiao-Dong . EDXD Study of α-LiIO₃ under High Pressure. Chinese Physics C, 2001, 25(S1): 62-65.
[19]	Chen Zhiqian , Zheng Renrong , Yin Chuanzong . Mössbauer Study of High T_c GdBa₂Cu₃O_7-δ. Chinese Physics C, 1992, 16(S2): 117-122.
[20]	Zheng Xite , Xu Yong . Analytic Study of SU(3) Lattice Gauge Theory. Chinese Physics C, 1989, 13(S3): 249-252.

Access

Get Citation

ZHANG Yu-Feng, LIU Jing, QIN Zhen-Xing, LIN Chuan-Long, XIONG Lun, LI Rui and BAI Li-Gang. A high-pressure study of PbCO₃ by XRD and Raman spectroscopy[J]. Chinese Physics C, 2013, 37(3): 038001. doi: 10.1088/1674-1137/37/3/038001

RIS(for EndNote,Reference Manager,ProCite)

BibTex

Txt

Milestone

Received: 2012-04-18
Revised: 2012-06-07

Article Metric

Article Views(1976)
PDF Downloads(398)
Cited by(0)

Policy on re-use

To reuse of subscription content published by CPC, the users need to request permission from CPC, unless the content was published under an Open Access license which automatically permits that type of reuse.

通讯作者: 陈斌, bchen63@163.com

1.
沈阳化工大学材料科学与工程学院沈阳 110142

A high-pressure study of PbCO₃ by XRD and Raman spectroscopy

Corresponding author: ZHANG Yu-Feng,

Corresponding author: LIU Jing,

Received Date: 2012-04-18

Accepted Date: 2012-06-07

Available Online: 2013-03-05

Abstract: The pressure-induced phase transitions of PbCO₃ are studied using synchrotron radiation in a diamond anvil cell at room temperature. The XRD measurement indicates that PbCO₃ with an initial phase of aragonite-type structure undergoes two phase transitions at ～ 7.8 GPa and ～ 15.7 GPa，respectively. The higher-pressure phase appearing at ～ 15.7 GPa is stable up to 51.8 GPa. The two phase transitions are further confirmed by Raman scattering up to 23.3 GPa. During the decompression process, the high-pressure phases of PbCO₃ are gradually recovered to the starting aragonite-type structure, but exhibit some hysteresis. The bulk modulus B₀ of the aragonite-type structure is obtained to be 63± (3) GPa by fitting the volume-pressure data to the Birch-Murnaghan equation of states with B₀' fixed to 4.

HTML

Reference (1)

A high-pressure study of PbCO₃ by XRD and Raman spectroscopy

Abstract：

References

Access

Article Metrics

Metrics

通讯作者: 陈斌, bchen63@163.com

Email This Article

A high-pressure study of PbCO₃ by XRD and Raman spectroscopy

Corresponding author: ZHANG Yu-Feng,

Corresponding author: LIU Jing,

HTML

目录

A high-pressure study of PbCO3 by XRD and Raman spectroscopy

Abstract：

References

Access

Article Metrics

Metrics

通讯作者: 陈斌, bchen63@163.com

Email This Article

A high-pressure study of PbCO3 by XRD and Raman spectroscopy

Corresponding author: ZHANG Yu-Feng,

Corresponding author: LIU Jing,

HTML

目录

A high-pressure study of PbCO₃ by XRD and Raman spectroscopy

A high-pressure study of PbCO₃ by XRD and Raman spectroscopy