XANES Investigation of Synthesized Nano-ZnO Capped by DDAB

JI Yun-Liang; HU Rong; WU Zi-Yu; GUO Lin; XU Hui-Bin; ZHANG Jing; XIE Ya-Ning; HU Tian-Dou

Chinese Physics C> 2003, Vol. 27> Issue(4) : 367-370

XANES Investigation of Synthesized Nano-ZnO Capped by DDAB

Department of Materials Science and Engineering, Beijing University of Astronauts and Astronautics, Beijing 100083, China2 Institute of High Energy Physics, CAS, Beijing 100039, China

Abstract
HTML
Reference
Related

PDF

Abstract：
Nano-sized semiconductors ZnO were synthesized with an upgraded reverse micelles by using DDAB (Didodecyldimethyl-ammounium bromide) as capped surfactants. The main advantage of this procedure is that the water needed to form micro reactors comes directly from intra molecule of Zn salt. The radius of nano-sized ZnO can be controlled by changing the concentration ratio of Zn salt and DDAB in organic solvent, and monitored by TEM images. XAFS spectroscopy is then used to recognize the distortion and the recombination on the surface of nanomaterial.

References

[1]

. ZHANG LiDe,MOU JiMei et al.Nanomaterials and Nanostructure.Beijing:Sciencepress,2001(in Chinese)(张立德,牟季美等.纳米材料和纳米结构.北京:科学出版社,2001)2. Kovtyukhova N I,Gorchinskiy A D et al.Materials Science and Engineering.2000,B69—70:424—430 3. Joshy Jose,Abdul Khadar M .Nano Structured Materials,1999,11(8):1091—10994. Monticone S ,Tufeu R ,Kanaev A V .J .Phys.Chem.,1998,B102:2854—2862 5. Mo C M ,LI Y H ,LIU Y S et al. J. Appl.Phys.,1998,83(8):43896. Lia J F ,Yaoa L Z ,Yea C H et al.Journal of Crystal Growth.,2001,223:535—538 7. Takuya Tsuzuki,Mc Cormic Paul G .Scripta Mater.,2001,44:1731—17348. WU Run,XIE ChangSheng,XIA Hui et al.Journal of Crystal Growth.,2000,217:274—280 9. GUO Lin,YANG ShiHe,YANG ChunLei et al.Appl.Phys.Lett.,2000,76:2901 10. Maurizio Olla,Maura Monduzzi,Luigi Ambrosone.Colloids and Surfaces A :Physicochemical and Engineering Aspects,1999,160:23—3611. ZHANG X T ,ZHUANG J Q ,REN Y L et al.ACTA Physico Chemica Sinica.,2000,16(7) 12. GUO Lin,YANG ShiHe. Applied Physics Letters.,2000,76(20)

[1]	LIU Li-Juan , LIU Hui-Jun , CUI Ming-Qi , HU Yong-Feng , ZHENG Lei , ZHAO Yi-Dong , MA Chen-Yan , XI Shi-Bo , YANG Dong-Liang , GUO Zhi-Ying , WANG Jie . Determination of the calcium species in coal chars by Ca K-edge XANES analysis. Chinese Physics C, 2013, 37(2): 028003. doi: 10.1088/1674-1137/37/2/028003
[2]	ZHENG Lei , ZHAO Yi-Dong , TANG Kun , MA Chen-Yan , HAN Yong , CUI Ming-Qi . Total electron yield mode for XANES measurements in the energy region of 2.1--6.0 keV. Chinese Physics C, 2011, 35(2): 199-202. doi: 10.1088/1674-1137/35/2/018
[3]	LIN Jun , BAO Liang-Man , LIU Wei , LI Yan , LI Yu-Lan , MA Chen-Yan , ZHAO Yi-Dong . Size distribution of sulfur species in fine and ultrafine aerosol particles using sulfur K-edge XANES. Chinese Physics C, 2009, 33(11): 965-968. doi: 10.1088/1674-1137/33/11/007
[4]	BAO Liang-Man , LIN Jun , LIU Wei , LU Wen-Zhong , ZHANG Gui-Lin , LI Yan , MA Chen-Yan , ZHAO Yi-Dong , HE Wei , HU Tian-Dou . Investigation of sulfur speciation in particles from small coal-burning boiler by XANES spectroscopy. Chinese Physics C, 2009, 33(11): 1001-1005. doi: 10.1088/1674-1137/33/11/014
[5]	BAO Liang-Man , ZHANG Gui-Lin , ZHANG Yuan-Xun , LI Yan , LIN Jun , LIU Wei , CAO Qing-Chen , ZHAO Yi-Dong , MA Chen-Yan , HAN Yong . Transfer characterization of sulfur from coal-burning emission to plant leaves by PIXE and XANES. Chinese Physics C, 2009, 33(11): 1010-1015. doi: 10.1088/1674-1137/33/11/016
[6]	ZHAO Ting , GAO Bin , LIU Lei , YE Qing , CHU Wang-Sheng , WU Zi-Yu . Theoretical XANES spectra for C₇₆ isomers. Chinese Physics C, 2009, 33(11): 954-959. doi: 10.1088/1674-1137/33/11/005
[7]	WANG Jia-Ou , DU Yong-Hua , Kurash Ibrahim , HONG Cai-Hao , XIE Ya-Ning , HU Tian-Dou . Study on Perovskite Oxides LaFe_1－xCr_xO₃ by EXAFS. Chinese Physics C, 2007, 31(1): 101-103.
[8]	GUO Xiao-Yun , CHU Wang-Sheng , GONG Wei-Min , DONG Yu-Hui , XIE Ya-Ning , YANG Fei-Fei , Maurizio Benfatto , WU Zi-Yu . MXAN Analysis of the XANES Energy Region of LiPDF. Chinese Physics C, 2007, 31(2): 199-203.
[9]	LIU Zu-Hua , BAO Jing-Dong . Synthesis and Decay of Superheavy Nuclei in the Deformed Region. Chinese Physics C, 2006, 30(S2): 118-120.
[10]	CHEN Dong-Liang , WU Zi-Yu , WEI Shi-Qiang . MS-XANES Studies on the Interface Effect of Semiconductor InSb Nanoparticles Embedded in a-SiO₂ Matrix. Chinese Physics C, 2006, 30(5): 476-480.
[11]	WANG Jia-Ou , KUI Re-Xi , WU Xiang , HONG Cai-Hao , ZHONG Jun , SU Run , QIAN Hai-Jie , WU Zi-Yu . Study of Electronic Structure in SrTi1-xRuxO3. Chinese Physics C, 2005, 29(S1): 47-50.
[12]	WANG Lin , LIU Bing-Bing , LIU De-Di , HOU Yuan-Yuan , YAO Ming-Guang , ZOU Guang-Tian , LI Hui , LUO Zong-Ju , LI YAN , LIU Jing . High Pressure Studies of Nano/Sub-Micrometer C70 Rods. Chinese Physics C, 2005, 29(S1): 112-115.
[13]	CHU Wang-Sheng , WU Zi-Yu , LIU Wen-Han . XANES Study of Hg Sorption Products on Montmorillonite at High Temperatures. Chinese Physics C, 2005, 29(S1): 84-88.
[14]	ZHONG Jun , LIU Chang , WU Zi-Yu , Mamatimin Abbas , KUI Re-Xi , CHENG Hui-Ming , GAO Bin , LIU Lei , , . XANES Study of Carbon Based Nanotubes. Chinese Physics C, 2005, 29(S1): 97-101.
[15]	HU Rong , WU Zi-Yu , LIU Jing , XIE Ya-Ning , HU Tian-Dou , ZHANG Jing , FENG Wei-Yue , CHAI Zhi-Fang . XANES Investigation of Chromium Valence State in Yeast Biomass. Chinese Physics C, 2004, 28(1): 100-103.
[16]	PAN Yue-Wu , QU Sheng-Chun , CUI Qi-Liang , ZHANG Wei-Wei , LIU Xi-Zhe , LIU Jing , LIU Bing-Bing , GAO Chun-Xiao , ZOU Guang-Tian . Pressure-Induced Phase Transition of Nanocrystalline Zinc Sulfide. Chinese Physics C, 2001, 25(S1): 58-61.
[17]	PENG Liang-Qiang , WANG Shi-Cheng , JU Xin , P.Yu.Apel , Masaru Yoshida . Fabrication of Nanoporous Nuclear Track Membranes. Chinese Physics C, 2001, 25(4): 359-364.
[18]	Xu Shuwei¹ , Li Zhankul¹ , Xie Yuanxiang¹ , Pan Qiangyan¹ , Yu Yong¹ , J.Adam² , Wang Chunfang¹ , king Jianping¹ , Hu Qingyuan¹ , Li Shihong¹ , Chen Hongyan¹ , Zhang Tianmei¹ , Jin Genming<sup . Six New Nuclides Near the Proton-drip Line in the Rare-earth Region. Chinese Physics C, 1999, 23(6): 589-593.
[19]	Xie Yuanxiang , Xu Shuwei , Li Zhankui , Ma Ruichang , Ge Yuanxiu , Wang Chunfang , Huang Wenxue , Zhang Tianmei . Synthesis and Study of the New β-delayed Proton Precursor Ce in the Region of Proton-drip Line. Chinese Physics C, 1997, 21(7): 668-671.
[20]	GU Yi-Fan , HE Jing-Tang , QIAN Zhong-Min , ZHU Guo-Yi , XU Yu-Heng , WAN Li-De , CHEN Gang , HE Zheng-Shu . A STUDY OF THE PROPERTIES OF ZINC TUNGSTATE FOR DETECTION OF PHOTONS. Chinese Physics C, 1988, 12(5): 577-580.

Access

Get Citation

JI Yun-Liang, HU Rong, WU Zi-Yu, GUO Lin, XU Hui-Bin, ZHANG Jing, XIE Ya-Ning and HU Tian-Dou. XANES Investigation of Synthesized Nano-ZnO Capped by DDAB[J]. Chinese Physics C, 2003, 27(4): 367-370.

JI Yun-Liang, HU Rong, WU Zi-Yu, GUO Lin, XU Hui-Bin, ZHANG Jing, XIE Ya-Ning and HU Tian-Dou. XANES Investigation of Synthesized Nano-ZnO Capped by DDAB[J]. Chinese Physics C, 2003, 27(4): 367-370. shu

RIS(for EndNote,Reference Manager,ProCite)

BibTex

Txt

Milestone

Received: 2002-06-14
Revised: 1900-01-01

Article Metric

Article Views(3128)
PDF Downloads(597)
Cited by(0)

Policy on re-use

To reuse of subscription content published by CPC, the users need to request permission from CPC, unless the content was published under an Open Access license which automatically permits that type of reuse.

通讯作者: 陈斌, bchen63@163.com

1.
沈阳化工大学材料科学与工程学院沈阳 110142

XANES Investigation of Synthesized Nano-ZnO Capped by DDAB

Corresponding author: WU Zi-Yu,

Department of Materials Science and Engineering, Beijing University of Astronauts and Astronautics, Beijing 100083, China2 Institute of High Energy Physics, CAS, Beijing 100039, China

Received Date: 2002-06-14

Accepted Date: 1900-01-01

Available Online: 2003-04-05

Abstract: Nano-sized semiconductors ZnO were synthesized with an upgraded reverse micelles by using DDAB (Didodecyldimethyl-ammounium bromide) as capped surfactants. The main advantage of this procedure is that the water needed to form micro reactors comes directly from intra molecule of Zn salt. The radius of nano-sized ZnO can be controlled by changing the concentration ratio of Zn salt and DDAB in organic solvent, and monitored by TEM images. XAFS spectroscopy is then used to recognize the distortion and the recombination on the surface of nanomaterial.

HTML

Reference (1)

XANES Investigation of Synthesized Nano-ZnO Capped by DDAB

Abstract：

References

Access

Article Metrics

Metrics

通讯作者: 陈斌, bchen63@163.com

Email This Article